| Rigaku R-AXIS RAPID-S diffractometer | 3799 independent reflections |
| Radiation source: fine-focus sealed tube | 3317 reflections with I > 2σ(I) |
| graphite | Rint = 0.071 |
| ω scans | θmax = 26.4°, θmin = 2.5° |
| Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | h = −9→9 |
| Tmin = 0.904, Tmax = 0.935 | k = −10→10 |
| 18356 measured reflections | l = −20→20 |
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