| Stoe IPDS-II diffractometer | 6956 independent reflections |
| Radiation source: fine-focus sealed tube | 4725 reflections with I > 2σ(I) |
| graphite | Rint = 0.080 |
| rotation method scans | θmax = 29.3°, θmin = 2.0° |
| Absorption correction: numerical (X-SHAPE; Stoe & Cie, 2005) | h = −22→22 |
| Tmin = 0.484, Tmax = 0.884 | k = −20→20 |
| 73587 measured reflections | l = −27→27 |
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