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. 2009 Feb 21;65(Pt 3):o553. doi: 10.1107/S1600536809004905
Bruker APEXII CCD area-detector diffractometer 2390 independent reflections
Radiation source: fine-focus sealed tube 1664 reflections with I > 2σ(I)
graphite Rint = 0.106
ω scans θmax = 25.3°, θmin = 2.0°
Absorption correction: multi-scan (SADABS; Bruker, 2006) h = −3→4
Tmin = 0.570, Tmax = 0.940 k = −12→12
13728 measured reflections l = −35→35