Bruker APEXII CCD area-detector diffractometer | 2390 independent reflections |
Radiation source: fine-focus sealed tube | 1664 reflections with I > 2σ(I) |
graphite | Rint = 0.106 |
ω scans | θmax = 25.3°, θmin = 2.0° |
Absorption correction: multi-scan (SADABS; Bruker, 2006) | h = −3→4 |
Tmin = 0.570, Tmax = 0.940 | k = −12→12 |
13728 measured reflections | l = −35→35 |