| Rigaku R-AXIS RAPID-II diffractometer | 2228 reflections with I > 2σ(I) |
| Detector resolution: 10.00 pixels mm-1 | Rint = 0.047 |
| ω scans | θmax = 30.0° |
| Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | h = −13→13 |
| Tmin = 0.847, Tmax = 0.880 | k = −27→27 |
| 9710 measured reflections | l = −8→9 |
| 3433 independent reflections |
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