3,4-Dimethyl­anilinium chloride monohydrate

. 2009 Feb 28;65(Pt 3):o628–o629. doi: 10.1107/S1600536809006072

O1W—H2W	0.81 (5)	C4—C5	1.378 (6)
O1W—H1W	0.80 (6)	C5—C6	1.382 (5)
N1—C1	1.477 (4)	C2—H2	0.9300
N1—H1A	0.8900	C5—H5	0.9300
N1—H1C	0.8900	C6—H6	0.9300
N1—H1B	0.8900	C7—H7B	0.9600
C1—C2	1.360 (5)	C7—H7C	0.9600
C1—C6	1.356 (5)	C7—H7A	0.9600
C2—C3	1.412 (5)	C8—H8C	0.9600
C3—C7	1.496 (6)	C8—H8A	0.9600
C3—C4	1.392 (5)	C8—H8B	0.9600
C4—C8	1.515 (5)

Cl1···O1W	3.217 (5)	C8···H7A	2.8400
Cl1···N1ⁱ	3.181 (4)	H1A···H2W	2.3400
Cl1···N1ⁱⁱ	3.177 (4)	H1A···O1W	1.8700
Cl1···O1Wⁱⁱⁱ	3.174 (5)	H1A···H6	2.3100
Cl1···H1W	2.43 (6)	H1A···H1W	2.4800
Cl1···H1Cⁱ	2.3100	H1B···Cl1^vi	2.3000
Cl1···H1Bⁱⁱ	2.3000	H1B···H2	2.4300
Cl1···H5^iv	3.0900	H1C···Cl1^vii	2.3100
Cl1···H2Wⁱⁱⁱ	2.36 (5)	H1W···H1A	2.4800
O1W···Cl1^v	3.174 (5)	H1W···Cl1	2.43 (6)
O1W···N1	2.754 (5)	H2···H1B	2.4300
O1W···Cl1	3.217 (5)	H2···H7B	2.3300
O1W···H1A	1.8700	H2W···Cl1^v	2.36 (5)
O1W···H6	2.9100	H2W···H1A	2.3400
N1···Cl1^vi	3.177 (4)	H5···H8A	2.3300
N1···Cl1^vii	3.181 (4)	H5···Cl1^viii	3.0900
N1···O1W	2.754 (5)	H6···H1A	2.3100
C3···C5^viii	3.509 (6)	H6···C7^xi	3.0800
C3···C4^viii	3.565 (6)	H6···O1W	2.9100
C4···C3^iv	3.565 (6)	H7A···H8B	2.4000
C4···C7^iv	3.570 (7)	H7A···C8	2.8400
C5···C3^iv	3.509 (6)	H7A···C3^viii	2.8400
C7···C4^viii	3.570 (7)	H7A···C4^viii	3.1000
C3···H7A^iv	2.8400	H7B···H2	2.3300
C4···H7A^iv	3.1000	H7C···C8	2.9300
C5···H7C^ix	3.0500	H7C···C5^xii	3.0500
C6···H7C^ix	2.9800	H7C···C6^xii	2.9800
C7···H8B	2.8100	H8A···H5	2.3300
C7···H8C	2.9500	H8B···C7	2.8100
C7···H6^x	3.0800	H8B···H7A	2.4000
C8···H7C	2.9300	H8C···C7	2.9500

H1W—O1W—H2W	110 (6)	C3—C2—H2	120.00
H1A—N1—H1B	109.00	C1—C2—H2	120.00
H1A—N1—H1C	109.00	C4—C5—H5	120.00
C1—N1—H1B	109.00	C6—C5—H5	119.00
C1—N1—H1C	109.00	C5—C6—H6	121.00
H1B—N1—H1C	109.00	C1—C6—H6	120.00
C1—N1—H1A	109.00	C3—C7—H7A	109.00
N1—C1—C2	119.3 (3)	C3—C7—H7B	109.00
C2—C1—C6	121.8 (3)	H7A—C7—H7B	109.00
N1—C1—C6	118.9 (3)	H7A—C7—H7C	109.00
C1—C2—C3	120.2 (3)	C3—C7—H7C	110.00
C2—C3—C4	118.1 (3)	H7B—C7—H7C	109.00
C2—C3—C7	119.5 (4)	C4—C8—H8B	109.00
C4—C3—C7	122.4 (3)	C4—C8—H8C	109.00
C3—C4—C8	119.8 (3)	C4—C8—H8A	109.00
C5—C4—C8	120.3 (3)	H8A—C8—H8C	109.00
C3—C4—C5	119.9 (3)	H8B—C8—H8C	109.00
C4—C5—C6	121.1 (3)	H8A—C8—H8B	110.00
C1—C6—C5	119.0 (3)

N1—C1—C2—C3	178.3 (3)	C2—C3—C4—C8	−179.7 (4)
C6—C1—C2—C3	−0.9 (6)	C7—C3—C4—C5	−179.6 (4)
N1—C1—C6—C5	−178.5 (3)	C7—C3—C4—C8	0.5 (6)
C2—C1—C6—C5	0.6 (6)	C3—C4—C5—C6	−0.4 (6)
C1—C2—C3—C4	0.4 (5)	C8—C4—C5—C6	179.5 (4)
C1—C2—C3—C7	−179.8 (4)	C4—C5—C6—C1	0.0 (6)
C2—C3—C4—C5	0.2 (5)