O1—C19 | 1.3688 (18) | C41—H412 | 0.99 |
O1—C2 | 1.3843 (19) | C42—C43 | 1.336 (2) |
C2—C3 | 1.343 (2) | C42—H42 | 0.95 |
C2—H2 | 0.95 | C43—C49 | 1.509 (2) |
C3—C13 | 1.454 (2) | C43—C44 | 1.512 (2) |
C3—H3 | 0.95 | C44—C45 | 1.537 (2) |
C4—O4 | 1.3613 (18) | C44—H441 | 0.99 |
C4—C13 | 1.407 (2) | C44—H442 | 0.99 |
C4—C14 | 1.416 (2) | C45—O5 | 1.4336 (19) |
C5—C6 | 1.349 (2) | C45—C46 | 1.504 (2) |
C5—C14 | 1.436 (2) | C45—H45 | 1.00 |
C5—H5 | 0.95 | O5—H51 | 0.84 |
C6—C7 | 1.447 (2) | C46—C47 | 1.337 (2) |
C6—H6 | 0.95 | C46—H46 | 0.95 |
C7—O7 | 1.2145 (19) | C47—C50 | 1.504 (2) |
C7—O8 | 1.3788 (19) | C47—C48 | 1.507 (2) |
O8—C18 | 1.3834 (18) | C48—H481 | 0.98 |
C9—C18 | 1.375 (2) | C48—H482 | 0.98 |
C9—C19 | 1.378 (2) | C48—H483 | 0.98 |
C9—H9 | 0.95 | C49—H491 | 0.98 |
C13—C19 | 1.413 (2) | C49—H492 | 0.98 |
C14—C18 | 1.413 (2) | C49—H493 | 0.98 |
O4—C41 | 1.4504 (17) | C50—H501 | 0.98 |
C41—C42 | 1.499 (2) | C50—H502 | 0.98 |
C41—H411 | 0.99 | C50—H503 | 0.98 |
C19—O1—C2 | 105.94 (12) | C43—C42—H42 | 116.7 |
C3—C2—O1 | 112.26 (14) | C41—C42—H42 | 116.7 |
C3—C2—H2 | 123.9 | C42—C43—C49 | 124.47 (14) |
O1—C2—H2 | 123.9 | C42—C43—C44 | 119.56 (14) |
C2—C3—C13 | 106.62 (14) | C49—C43—C44 | 115.95 (13) |
C2—C3—H3 | 126.7 | C43—C44—C45 | 113.08 (13) |
C13—C3—H3 | 126.7 | C43—C44—H441 | 109.0 |
O4—C4—C13 | 126.59 (13) | C45—C44—H441 | 109.0 |
O4—C4—C14 | 114.47 (13) | C43—C44—H442 | 109.0 |
C13—C4—C14 | 118.94 (13) | C45—C44—H442 | 109.0 |
C6—C5—C14 | 121.15 (14) | H441—C44—H442 | 107.8 |
C6—C5—H5 | 119.4 | O5—C45—C46 | 106.58 (13) |
C14—C5—H5 | 119.4 | O5—C45—C44 | 111.88 (13) |
C5—C6—C7 | 121.23 (15) | C46—C45—C44 | 110.45 (13) |
C5—C6—H6 | 119.4 | O5—C45—H45 | 109.3 |
C7—C6—H6 | 119.4 | C46—C45—H45 | 109.3 |
O7—C7—O8 | 116.20 (14) | C44—C45—H45 | 109.3 |
O7—C7—C6 | 126.77 (15) | C45—O5—H51 | 109.5 |
O8—C7—C6 | 117.03 (13) | C47—C46—C45 | 127.87 (15) |
C7—O8—C18 | 122.82 (12) | C47—C46—H46 | 116.1 |
C18—C9—C19 | 114.72 (14) | C45—C46—H46 | 116.1 |
C18—C9—H9 | 122.6 | C46—C47—C50 | 125.44 (16) |
C19—C9—H9 | 122.6 | C46—C47—C48 | 120.82 (15) |
C4—C13—C19 | 117.12 (13) | C50—C47—C48 | 113.73 (15) |
C4—C13—C3 | 138.18 (14) | C47—C48—H481 | 109.5 |
C19—C13—C3 | 104.68 (13) | C47—C48—H482 | 109.5 |
C18—C14—C4 | 119.34 (13) | H481—C48—H482 | 109.5 |
C18—C14—C5 | 117.56 (13) | C47—C48—H483 | 109.5 |
C4—C14—C5 | 123.09 (13) | H481—C48—H483 | 109.5 |
C9—C18—O8 | 116.11 (13) | H482—C48—H483 | 109.5 |
C9—C18—C14 | 123.71 (14) | C43—C49—H491 | 109.5 |
O8—C18—C14 | 120.18 (13) | C43—C49—H492 | 109.5 |
O1—C19—C9 | 123.36 (14) | H491—C49—H492 | 109.5 |
O1—C19—C13 | 110.49 (13) | C43—C49—H493 | 109.5 |
C9—C19—C13 | 126.15 (14) | H491—C49—H493 | 109.5 |
C4—O4—C41 | 119.53 (11) | H492—C49—H493 | 109.5 |
O4—C41—C42 | 105.47 (12) | C47—C50—H501 | 109.5 |
O4—C41—H411 | 110.6 | C47—C50—H502 | 109.5 |
C42—C41—H411 | 110.6 | H501—C50—H502 | 109.5 |
O4—C41—H412 | 110.6 | C47—C50—H503 | 109.5 |
C42—C41—H412 | 110.6 | H501—C50—H503 | 109.5 |
H411—C41—H412 | 108.8 | H502—C50—H503 | 109.5 |
C43—C42—C41 | 126.62 (14) | ||
C19—O1—C2—C3 | 0.41 (17) | C4—C14—C18—O8 | 179.09 (12) |
O1—C2—C3—C13 | 0.19 (18) | C5—C14—C18—O8 | −1.7 (2) |
C14—C5—C6—C7 | 0.2 (2) | C2—O1—C19—C9 | 178.89 (14) |
C5—C6—C7—O7 | 179.33 (15) | C2—O1—C19—C13 | −0.87 (16) |
C5—C6—C7—O8 | −0.2 (2) | C18—C9—C19—O1 | −178.88 (13) |
O7—C7—O8—C18 | 179.60 (13) | C18—C9—C19—C13 | 0.9 (2) |
C6—C7—O8—C18 | −0.8 (2) | C4—C13—C19—O1 | 179.76 (12) |
O4—C4—C13—C19 | 177.50 (13) | C3—C13—C19—O1 | 0.98 (16) |
C14—C4—C13—C19 | −1.4 (2) | C4—C13—C19—C9 | 0.0 (2) |
O4—C4—C13—C3 | −4.3 (3) | C3—C13—C19—C9 | −178.78 (14) |
C14—C4—C13—C3 | 176.88 (16) | C13—C4—O4—C41 | −3.8 (2) |
C2—C3—C13—C4 | −179.08 (17) | C14—C4—O4—C41 | 175.09 (12) |
C2—C3—C13—C19 | −0.70 (16) | C4—O4—C41—C42 | −166.21 (12) |
O4—C4—C14—C18 | −177.18 (12) | O4—C41—C42—C43 | 141.31 (15) |
C13—C4—C14—C18 | 1.8 (2) | C41—C42—C43—C49 | 2.1 (2) |
O4—C4—C14—C5 | 3.7 (2) | C41—C42—C43—C44 | −176.19 (14) |
C13—C4—C14—C5 | −177.31 (13) | C42—C43—C44—C45 | 113.54 (16) |
C6—C5—C14—C18 | 0.8 (2) | C49—C43—C44—C45 | −64.89 (17) |
C6—C5—C14—C4 | 179.90 (14) | C43—C44—C45—O5 | −53.12 (17) |
C19—C9—C18—O8 | 179.60 (12) | C43—C44—C45—C46 | −171.68 (13) |
C19—C9—C18—C14 | −0.4 (2) | O5—C45—C46—C47 | 109.83 (18) |
C7—O8—C18—C9 | −178.14 (13) | C44—C45—C46—C47 | −128.43 (17) |
C7—O8—C18—C14 | 1.8 (2) | C45—C46—C47—C50 | −0.7 (3) |
C4—C14—C18—C9 | −0.9 (2) | C45—C46—C47—C48 | 179.69 (15) |
C5—C14—C18—C9 | 178.22 (14) |