| Nonius KappaCCD diffractometer | 5819 independent reflections |
| Radiation source: fine-focus sealed tube | 3804 reflections with I > 2σ(I) |
| graphite | Rint = 0.080 |
| Detector resolution: 9 pixels mm-1 | θmax = 25.0°, θmin = 1.9° |
| CCD rotation images, thick slices scans | h = −7→9 |
| Absorption correction: multi-scan (Blessing, 1995) | k = −12→13 |
| Tmin = 0.864, Tmax = 0.988 | l = −21→23 |
| 13842 measured reflections |
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