| Bruker SMART CCD area-detector diffractometer | 1356 independent reflections |
| Radiation source: fine-focus sealed tube | 1204 reflections with I > 2σ(I) |
| graphite | Rint = 0.017 |
| φ and ω scans | θmax = 25.0°, θmin = 3.0° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −9→8 |
| Tmin = 0.757, Tmax = 0.897 | k = −15→15 |
| 4287 measured reflections | l = −8→8 |
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