| Bruker SMART APEXII CCD area-detector diffractometer | 2954 independent reflections |
| Radiation source: fine-focus sealed tube | 2157 reflections with I > 2σ(I) |
| graphite | Rint = 0.033 |
| φ and ω scans | θmax = 30.4°, θmin = 1.9° |
| Absorption correction: multi-scan (SADABS; Bruker, 2005) | h = −9→9 |
| Tmin = 0.961, Tmax = 0.994 | k = −9→9 |
| 8962 measured reflections | l = −14→15 |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.