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. 2009 Mar 6;65(Pt 4):o706. doi: 10.1107/S1600536809007545
Refinement on F2 Primary atom site location: structure-invariant direct methods
Least-squares matrix: full Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.049 Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.131 H-atom parameters constrained
S = 1.04 w = 1/[σ2(Fo2) + (0.0681P)2 + 0.047P] where P = (Fo2 + 2Fc2)/3
2954 reflections (Δ/σ)max < 0.001
129 parameters Δρmax = 0.43 e Å3
0 restraints Δρmin = −0.27 e Å3