Br1—C5 | 1.901 (5) | C12—H12 | 0.9300 |
Br2—C20 | 1.886 (5) | C13—C14 | 1.381 (7) |
O1—C2 | 1.358 (5) | C13—H13 | 0.9300 |
O1—C32 | 1.431 (6) | C14—H14 | 0.9300 |
O2—C8 | 1.223 (5) | C15—H15A | 0.9600 |
O3—C11 | 1.369 (5) | C15—H15B | 0.9600 |
O3—C15 | 1.426 (6) | C15—H15C | 0.9600 |
O4—C17 | 1.363 (5) | C16—C21 | 1.386 (6) |
O4—C31 | 1.438 (5) | C16—C17 | 1.405 (6) |
O5—C23 | 1.219 (5) | C16—C22 | 1.460 (6) |
O6—C26 | 1.376 (6) | C17—C18 | 1.388 (6) |
O6—C30 | 1.414 (6) | C18—C19 | 1.376 (6) |
N1—C7 | 1.267 (5) | C18—H18 | 0.9300 |
N1—N2 | 1.380 (5) | C19—C20 | 1.378 (6) |
N2—C8 | 1.353 (5) | C19—H19 | 0.9300 |
N2—H2 | 0.90 (3) | C20—C21 | 1.383 (6) |
N3—C22 | 1.275 (5) | C21—H21 | 0.9300 |
N3—N4 | 1.377 (4) | C22—H22 | 0.9300 |
N4—C23 | 1.339 (5) | C23—C24 | 1.503 (6) |
N4—H4A | 0.90 (3) | C24—C29 | 1.371 (6) |
C1—C6 | 1.388 (6) | C24—C25 | 1.386 (6) |
C1—C2 | 1.414 (6) | C25—C26 | 1.399 (6) |
C1—C7 | 1.470 (6) | C25—H25 | 0.9300 |
C2—C3 | 1.382 (6) | C26—C27 | 1.391 (7) |
C3—C4 | 1.377 (6) | C27—C28 | 1.348 (7) |
C3—H3 | 0.9300 | C27—H27 | 0.9300 |
C4—C5 | 1.372 (6) | C28—C29 | 1.377 (7) |
C4—H4 | 0.9300 | C28—H28 | 0.9300 |
C5—C6 | 1.370 (6) | C29—H29 | 0.9300 |
C6—H6 | 0.9300 | C30—H30A | 0.9600 |
C7—H7 | 0.9300 | C30—H30B | 0.9600 |
C8—C9 | 1.494 (6) | C30—H30C | 0.9600 |
C9—C14 | 1.367 (6) | C31—H31A | 0.9600 |
C9—C10 | 1.397 (6) | C31—H31B | 0.9600 |
C10—C11 | 1.384 (6) | C31—H31C | 0.9600 |
C10—H10 | 0.9300 | C32—H32A | 0.9600 |
C11—C12 | 1.393 (7) | C32—H32B | 0.9600 |
C12—C13 | 1.336 (7) | C32—H32C | 0.9600 |
C2—O1—C32 | 118.2 (4) | C21—C16—C17 | 118.5 (4) |
C11—O3—C15 | 116.7 (4) | C21—C16—C22 | 121.7 (4) |
C17—O4—C31 | 118.0 (4) | C17—C16—C22 | 119.8 (4) |
C26—O6—C30 | 118.2 (4) | O4—C17—C18 | 124.2 (4) |
C7—N1—N2 | 114.8 (4) | O4—C17—C16 | 115.8 (4) |
C8—N2—N1 | 119.3 (4) | C18—C17—C16 | 120.1 (4) |
C8—N2—H2 | 122 (4) | C19—C18—C17 | 120.5 (4) |
N1—N2—H2 | 119 (4) | C19—C18—H18 | 119.7 |
C22—N3—N4 | 114.2 (3) | C17—C18—H18 | 119.7 |
C23—N4—N3 | 119.1 (3) | C18—C19—C20 | 119.7 (4) |
C23—N4—H4A | 117 (3) | C18—C19—H19 | 120.2 |
N3—N4—H4A | 123 (3) | C20—C19—H19 | 120.2 |
C6—C1—C2 | 119.2 (4) | C19—C20—C21 | 120.5 (4) |
C6—C1—C7 | 121.8 (4) | C19—C20—Br2 | 119.2 (3) |
C2—C1—C7 | 119.0 (4) | C21—C20—Br2 | 120.4 (4) |
O1—C2—C3 | 124.8 (4) | C20—C21—C16 | 120.8 (4) |
O1—C2—C1 | 116.0 (4) | C20—C21—H21 | 119.6 |
C3—C2—C1 | 119.2 (5) | C16—C21—H21 | 119.6 |
C4—C3—C2 | 120.6 (5) | N3—C22—C16 | 120.8 (4) |
C4—C3—H3 | 119.7 | N3—C22—H22 | 119.6 |
C2—C3—H3 | 119.7 | C16—C22—H22 | 119.6 |
C5—C4—C3 | 119.8 (4) | O5—C23—N4 | 123.5 (4) |
C5—C4—H4 | 120.1 | O5—C23—C24 | 120.6 (4) |
C3—C4—H4 | 120.1 | N4—C23—C24 | 115.9 (4) |
C6—C5—C4 | 121.2 (4) | C29—C24—C25 | 120.1 (4) |
C6—C5—Br1 | 119.4 (4) | C29—C24—C23 | 119.9 (4) |
C4—C5—Br1 | 119.4 (4) | C25—C24—C23 | 119.8 (4) |
C5—C6—C1 | 119.9 (4) | C24—C25—C26 | 119.5 (4) |
C5—C6—H6 | 120.0 | C24—C25—H25 | 120.2 |
C1—C6—H6 | 120.0 | C26—C25—H25 | 120.2 |
N1—C7—C1 | 119.4 (4) | O6—C26—C27 | 116.1 (4) |
N1—C7—H7 | 120.3 | O6—C26—C25 | 124.1 (5) |
C1—C7—H7 | 120.3 | C27—C26—C25 | 119.8 (5) |
O2—C8—N2 | 122.6 (4) | C28—C27—C26 | 118.8 (5) |
O2—C8—C9 | 122.1 (4) | C28—C27—H27 | 120.6 |
N2—C8—C9 | 115.0 (4) | C26—C27—H27 | 120.6 |
C14—C9—C10 | 119.9 (4) | C27—C28—C29 | 122.7 (5) |
C14—C9—C8 | 124.9 (4) | C27—C28—H28 | 118.7 |
C10—C9—C8 | 115.2 (4) | C29—C28—H28 | 118.7 |
C11—C10—C9 | 119.3 (4) | C24—C29—C28 | 119.1 (5) |
C11—C10—H10 | 120.4 | C24—C29—H29 | 120.4 |
C9—C10—H10 | 120.4 | C28—C29—H29 | 120.4 |
O3—C11—C10 | 124.0 (5) | O6—C30—H30A | 109.5 |
O3—C11—C12 | 117.0 (5) | O6—C30—H30B | 109.5 |
C10—C11—C12 | 119.0 (5) | H30A—C30—H30B | 109.5 |
C13—C12—C11 | 121.0 (5) | O6—C30—H30C | 109.5 |
C13—C12—H12 | 119.5 | H30A—C30—H30C | 109.5 |
C11—C12—H12 | 119.5 | H30B—C30—H30C | 109.5 |
C12—C13—C14 | 120.6 (5) | O4—C31—H31A | 109.5 |
C12—C13—H13 | 119.7 | O4—C31—H31B | 109.5 |
C14—C13—H13 | 119.7 | H31A—C31—H31B | 109.5 |
C9—C14—C13 | 120.0 (5) | O4—C31—H31C | 109.5 |
C9—C14—H14 | 120.0 | H31A—C31—H31C | 109.5 |
C13—C14—H14 | 120.0 | H31B—C31—H31C | 109.5 |
O3—C15—H15A | 109.5 | O1—C32—H32A | 109.5 |
O3—C15—H15B | 109.5 | O1—C32—H32B | 109.5 |
H15A—C15—H15B | 109.5 | H32A—C32—H32B | 109.5 |
O3—C15—H15C | 109.5 | O1—C32—H32C | 109.5 |
H15A—C15—H15C | 109.5 | H32A—C32—H32C | 109.5 |
H15B—C15—H15C | 109.5 | H32B—C32—H32C | 109.5 |
C7—N1—N2—C8 | 167.8 (4) | C12—C13—C14—C9 | −0.8 (9) |
C22—N3—N4—C23 | 175.4 (4) | C31—O4—C17—C18 | 1.9 (6) |
C32—O1—C2—C3 | 4.8 (7) | C31—O4—C17—C16 | −177.7 (4) |
C32—O1—C2—C1 | −175.0 (4) | C21—C16—C17—O4 | 179.0 (4) |
C6—C1—C2—O1 | 179.4 (4) | C22—C16—C17—O4 | −3.4 (6) |
C7—C1—C2—O1 | −1.3 (6) | C21—C16—C17—C18 | −0.6 (6) |
C6—C1—C2—C3 | −0.4 (7) | C22—C16—C17—C18 | 177.0 (4) |
C7—C1—C2—C3 | 178.9 (4) | O4—C17—C18—C19 | −179.5 (4) |
O1—C2—C3—C4 | 179.0 (4) | C16—C17—C18—C19 | 0.1 (7) |
C1—C2—C3—C4 | −1.2 (7) | C17—C18—C19—C20 | 0.9 (7) |
C2—C3—C4—C5 | 1.8 (7) | C18—C19—C20—C21 | −1.4 (7) |
C3—C4—C5—C6 | −0.7 (7) | C18—C19—C20—Br2 | 178.5 (3) |
C3—C4—C5—Br1 | 178.7 (4) | C19—C20—C21—C16 | 0.8 (7) |
C4—C5—C6—C1 | −1.0 (7) | Br2—C20—C21—C16 | −179.1 (3) |
Br1—C5—C6—C1 | 179.7 (3) | C17—C16—C21—C20 | 0.2 (6) |
C2—C1—C6—C5 | 1.5 (7) | C22—C16—C21—C20 | −177.3 (4) |
C7—C1—C6—C5 | −177.8 (4) | N4—N3—C22—C16 | 177.8 (3) |
N2—N1—C7—C1 | 177.6 (4) | C21—C16—C22—N3 | −18.1 (6) |
C6—C1—C7—N1 | −18.0 (6) | C17—C16—C22—N3 | 164.4 (4) |
C2—C1—C7—N1 | 162.7 (4) | N3—N4—C23—O5 | 0.1 (6) |
N1—N2—C8—O2 | −3.9 (6) | N3—N4—C23—C24 | −177.8 (3) |
N1—N2—C8—C9 | −177.8 (3) | O5—C23—C24—C29 | 38.0 (6) |
O2—C8—C9—C14 | 143.8 (5) | N4—C23—C24—C29 | −144.0 (4) |
N2—C8—C9—C14 | −42.3 (6) | O5—C23—C24—C25 | −136.1 (5) |
O2—C8—C9—C10 | −36.7 (6) | N4—C23—C24—C25 | 41.9 (6) |
N2—C8—C9—C10 | 137.2 (4) | C29—C24—C25—C26 | −0.9 (7) |
C14—C9—C10—C11 | 3.5 (7) | C23—C24—C25—C26 | 173.2 (4) |
C8—C9—C10—C11 | −176.1 (4) | C30—O6—C26—C27 | 179.4 (5) |
C15—O3—C11—C10 | −7.5 (8) | C30—O6—C26—C25 | −0.7 (7) |
C15—O3—C11—C12 | 171.5 (5) | C24—C25—C26—O6 | −178.0 (4) |
C9—C10—C11—O3 | 176.1 (4) | C24—C25—C26—C27 | 1.8 (7) |
C9—C10—C11—C12 | −2.8 (7) | O6—C26—C27—C28 | 178.8 (5) |
O3—C11—C12—C13 | −178.7 (5) | C25—C26—C27—C28 | −1.0 (8) |
C10—C11—C12—C13 | 0.3 (8) | C26—C27—C28—C29 | −0.8 (9) |
C11—C12—C13—C14 | 1.5 (9) | C25—C24—C29—C28 | −0.9 (7) |
C10—C9—C14—C13 | −1.7 (8) | C23—C24—C29—C28 | −174.9 (5) |
C8—C9—C14—C13 | 177.8 (5) | C27—C28—C29—C24 | 1.7 (9) |