Table 1. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| O3—H3⋯O2i | 0.870 (11) | 1.802 (12) | 2.6680 (14) | 173.2 (16) |
| N1—H1NA⋯O1 | 0.884 (13) | 2.271 (14) | 3.0466 (19) | 146.3 (16) |
| N1—H1NB⋯N4ii | 0.879 (13) | 2.151 (13) | 3.0287 (19) | 177.3 (17) |
| N2—H2NA⋯O3 | 0.889 (15) | 2.093 (15) | 2.8333 (16) | 140.2 (14) |
| N2—H2NA⋯O1 | 0.889 (15) | 2.190 (15) | 2.9497 (18) | 143.2 (14) |
| N3—H3NA⋯O1Wiii | 0.872 (14) | 2.261 (19) | 2.8609 (18) | 125.9 (15) |
| N3—H3NA⋯O3 | 0.872 (14) | 2.573 (16) | 3.2241 (18) | 132.2 (16) |
| N3—H3NB⋯N6iv | 0.900 (14) | 2.133 (14) | 3.0313 (19) | 176.2 (18) |
| N5—H5NA⋯O1Wv | 0.901 (13) | 1.940 (14) | 2.8148 (16) | 163.2 (15) |
| N5—H5NB⋯O2vi | 0.895 (13) | 2.153 (15) | 2.9581 (16) | 149.4 (15) |
| O1W—H1WA⋯O1 | 0.858 (14) | 1.852 (14) | 2.6861 (16) | 163.8 (17) |
| O1W—H1WB⋯O2vii | 0.804 (13) | 2.297 (15) | 2.9738 (17) | 142.3 (17) |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
.