| Siemens SMART CCD diffractometer | 3310 independent reflections |
| Radiation source: fine-focus sealed tube | 2319 reflections with I > 2σ(I) |
| graphite | Rint = 0.050 |
| ω scans | θmax = 25.0°, θmin = 1.8° |
| Absorption correction: multi-scan (SADABS; Siemens, 1996) | h = −28→27 |
| Tmin = 0.566, Tmax = 0.615 | k = −14→15 |
| 9477 measured reflections | l = −13→15 |
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