| Nonius KappaCCD diffractometer | 2085 reflections with I > 2σ(I) |
| Radiation source: rotating anode | Rint = 0.049 |
| MONTEL, graded multilayered X-ray optics | θmax = 27.5°, θmin = 3.2° |
| Detector resolution: 9 pixels mm-1 | h = −11→11 |
| CCD; rotation images; thick slices scans | k = −18→18 |
| 7575 measured reflections | l = −17→17 |
| 3893 independent reflections |
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