| Bruker SMART APEX diffractometer | 1965 independent reflections |
| Radiation source: fine-focus sealed tube | 1952 reflections with I > 2σ(I) |
| graphite | Rint = 0.011 |
| ω scans | θmax = 27.5°, θmin = 3.0° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −8→8 |
| Tmin = 0.858, Tmax = 0.949 | k = −8→8 |
| 2247 measured reflections | l = −9→9 |