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. 2009 Jun 10;65(Pt 7):o1543–o1544. doi: 10.1107/S1600536809021436
Oxford Diffraction Xcalibur Ruby diffractometer 6334 independent reflections
Radiation source: Enhance (Cu) X-ray Source 6050 reflections with I > 2σ(I)
graphite Rint = 0.024
Detector resolution: 10.2576 pixels mm-1 θmax = 75.6°, θmin = 3.9°
ω scans h = −15→9
Absorption correction: multi-scan (CrysAlis PRO; Oxford Diffraction, 2009) k = −19→19
Tmin = 0.767, Tmax = 0.811 l = −21→21
11111 measured reflections