Oxford Diffraction Xcalibur Ruby diffractometer | 6334 independent reflections |
Radiation source: Enhance (Cu) X-ray Source | 6050 reflections with I > 2σ(I) |
graphite | Rint = 0.024 |
Detector resolution: 10.2576 pixels mm-1 | θmax = 75.6°, θmin = 3.9° |
ω scans | h = −15→9 |
Absorption correction: multi-scan (CrysAlis PRO; Oxford Diffraction, 2009) | k = −19→19 |
Tmin = 0.767, Tmax = 0.811 | l = −21→21 |
11111 measured reflections |