| Bruker APEXII CCD area-detector diffractometer | 7416 independent reflections | 
| Radiation source: sealed tube | 7177 reflections with I > 2σ(I) | 
| graphite | Rint = 0.028 | 
| φ and ω scans | θmax = 37.5°, θmin = 2.2° | 
| Absorption correction: multi-scan (SADABS; Bruker, 2005) | h = −43→43 | 
| Tmin = 0.872, Tmax = 0.951 | k = −6→6 | 
| 56940 measured reflections | l = −23→24 |