Bruker APEXII CCD area-detector diffractometer | 7416 independent reflections |
Radiation source: sealed tube | 7177 reflections with I > 2σ(I) |
graphite | Rint = 0.028 |
φ and ω scans | θmax = 37.5°, θmin = 2.2° |
Absorption correction: multi-scan (SADABS; Bruker, 2005) | h = −43→43 |
Tmin = 0.872, Tmax = 0.951 | k = −6→6 |
56940 measured reflections | l = −23→24 |