| Bruker SMART APEX CCD diffractometer | 2837 independent reflections |
| Radiation source: sealed tube | 2432 reflections with I > 2σ(I) |
| graphite | Rint = 0.059 |
| φ and ω scans | θmax = 26.0°, θmin = 1.8° |
| Absorption correction: multi-scan (SADABS; Bruker, 2000) | h = −9→8 |
| Tmin = 0.97, Tmax = 0.98 | k = −15→15 |
| 13853 measured reflections | l = −27→30 |
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