| Bruker SMART APEXII CCD area-detector diffractometer | 5318 independent reflections |
| Radiation source: fine-focus sealed tube | 4128 reflections with I > 2σ(I) |
| graphite | Rint = 0.032 |
| φ and ω scans | θmax = 30.1°, θmin = 1.4° |
| Absorption correction: multi-scan (SADABS; Bruker, 2005) | h = −41→41 |
| Tmin = 0.862, Tmax = 0.983 | k = −11→11 |
| 40913 measured reflections | l = −21→18 |