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. 2009 Jun 6;65(Pt 7):o1525–o1526. doi: 10.1107/S1600536809020595
P1A—C1A 1.836 (4) P1B—C1B 1.8258
P1A—C7A 1.833 (3) P1B—C7B 1.831 (3)
P1A—C13A 1.829 (3) P1B—C13B 1.831 (3)
O1A—C2A 1.362 (6) O1B—C2B 1.3767
O1A—C19A 1.440 (4) O1B—C19B 1.397 (4)
O2A—C20A 1.348 (5) O2B—C8B 1.383 (3)
O2A—C8A 1.373 (6) O2B—C20B 1.419 (4)
O3A—C14A 1.392 (5) O3B—C14B 1.379 (5)
O3A—C21A 1.411 (3) O3B—C21B 1.390 (6)
C1A—C2A 1.393 (5) C1B—C2B 1.400
C1A—C6A 1.400 (5) C1B—C6B 1.403 (3)
C2A—C3A 1.399 (6) C2B—C3B 1.3914
C3A—C4A 1.356 (7) C3B—C4B 1.357 (5)
C3A—H3A 0.93 C3B—H3B 0.93
C4A—C5A 1.375 (8) C4B—C5B 1.381 (9)
C4A—H4A 0.93 C4B—H4B 0.93
C5A—C6A 1.392 (6) C5B—C6B 1.386 (6)
C5A—H5A 0.93 C5B—H5B 0.93
C6A—H6A 0.93 C6B—H6B 0.93
C7A—C8A 1.388 (5) C7B—C12B 1.395 (5)
C7A—C12A 1.394 (4) C7B—C8B 1.402 (4)
C8A—C9A 1.379 (7) C8B—C9B 1.383 (5)
C9A—C10A 1.375 (9) C9B—C10B 1.400 (6)
C9A—H9A 0.93 C9B—H9B 0.93
C10A—C11A 1.390 (8) C10B—C11B 1.465 (5)
C10A—H10A 0.93 C10B—H10B 0.93
C11A—C12A 1.396 (5) C11B—C12B 1.377 (7)
C11A—H11A 0.93 C11B—H11B 0.93
C12A—H12A 0.93 C12B—H12B 0.93
C13A—C18A 1.391 (5) C13B—C18B 1.386 (5)
C13A—C14A 1.406 (5) C13B—C14B 1.386 (4)
C14A—C15A 1.385 (6) C14B—C15B 1.385 (7)
C15A—C16A 1.375 (7) C15B—C16B 1.385 (8)
C15A—H15A 0.93 C15B—H15B 0.93
C16A—C17A 1.421 (6) C16B—C17B 1.392 (6)
C16A—H16A 0.93 C16B—H16B 0.93
C17A—C18A 1.437 (6) C17B—C18B 1.389 (6)
C17A—H17A 0.93 C17B—H17B 0.93
C18A—H18A 0.93 C18B—H18B 0.93
C19A—H19A 0.96 C19B—H19D 0.96
C19A—H19B 0.96 C19B—H19E 0.96
C19A—H19C 0.96 C19B—H19F 0.96
C20A—H20A 0.96 C20B—H20D 0.96
C20A—H20B 0.96 C20B—H20E 0.96
C20A—H20C 0.96 C20B—H20F 0.96
C21A—H21A 0.96 C21B—H21D 0.96
C21A—H21B 0.96 C21B—H21E 0.96
C21A—H21C 0.96 C21B—H21F 0.96
C7A—P1A—C1A 101.47 (14) O1B—C2B—C3B 124.3
C13A—P1A—C1A 101.57 (15) O1B—C2B—C1B 115.3
C13A—P1A—C7A 102.02 (15) C3B—C2B—C1B 120.4
C2A—O1A—C19A 117.8 (5) C4B—C3B—C2B 121.44 (16)
C20A—O2A—C8A 113.4 (4) C4B—C3B—H3B 119.3
C14A—O3A—C21A 117.6 (3) C2B—C3B—H3B 119.3
C2A—C1A—C6A 117.8 (3) C3B—C4B—C5B 119.8 (3)
C2A—C1A—P1A 118.5 (3) C3B—C4B—H4B 120.1
C6A—C1A—P1A 123.5 (3) C5B—C4B—H4B 120.1
O1A—C2A—C1A 114.8 (3) C4B—C5B—C6B 119.4 (5)
O1A—C2A—C3A 124.5 (4) C4B—C5B—H5B 120.3
C1A—C2A—C3A 120.7 (4) C6B—C5B—H5B 120.3
C4A—C3A—C2A 120.0 (4) C5B—C6B—C1B 122.1 (4)
C4A—C3A—H3A 120.0 C5B—C6B—H6B 118.9
C2A—C3A—H3A 120.0 C1B—C6B—H6B 118.9
C3A—C4A—C5A 120.9 (4) C12B—C7B—C8B 116.9 (3)
C3A—C4A—H4A 119.5 C12B—C7B—P1B 124.3 (3)
C5A—C4A—H4A 119.5 C8B—C7B—P1B 118.7 (2)
C4A—C5A—C6A 119.6 (5) C9B—C8B—O2B 123.1 (3)
C4A—C5A—H5A 120.2 C9B—C8B—C7B 122.8 (3)
C6A—C5A—H5A 120.2 O2B—C8B—C7B 114.1 (3)
C5A—C6A—C1A 120.8 (4) C8B—C9B—C10B 118.1 (4)
C5A—C6A—H6A 119.6 C8B—C9B—H9B 121.0
C1A—C6A—H6A 119.6 C10B—C9B—H9B 121.0
C8A—C7A—C12A 117.8 (3) C9B—C10B—C11B 122.2 (4)
C8A—C7A—P1A 117.6 (3) C9B—C10B—H10B 118.9
C12A—C7A—P1A 124.2 (3) C11B—C10B—H10B 118.9
O2A—C8A—C9A 123.3 (5) C12B—C11B—C10B 114.4 (5)
O2A—C8A—C7A 115.1 (4) C12B—C11B—H11B 122.8
C9A—C8A—C7A 121.6 (5) C10B—C11B—H11B 122.8
C10A—C9A—C8A 119.9 (6) C11B—C12B—C7B 125.5 (4)
C10A—C9A—H9A 120.1 C11B—C12B—H12B 117.3
C8A—C9A—H9A 120.1 C7B—C12B—H12B 117.3
C9A—C10A—C11A 120.5 (4) C18B—C13B—C14B 117.1 (3)
C9A—C10A—H10A 119.7 C18B—C13B—P1B 124.9 (2)
C11A—C10A—H10A 119.7 C14B—C13B—P1B 117.9 (3)
C10A—C11A—C12A 118.8 (5) O3B—C14B—C15B 123.5 (3)
C10A—C11A—H11A 120.6 O3B—C14B—C13B 114.4 (3)
C12A—C11A—H11A 120.6 C15B—C14B—C13B 122.0 (4)
C7A—C12A—C11A 121.4 (4) C16B—C15B—C14B 119.7 (4)
C7A—C12A—H12A 119.3 C16B—C15B—H15B 120.2
C11A—C12A—H12A 119.3 C14B—C15B—H15B 120.2
C18A—C13A—C14A 116.7 (3) C15B—C16B—C17B 119.8 (4)
C18A—C13A—P1A 124.0 (3) C15B—C16B—H16B 120.1
C14A—C13A—P1A 119.0 (3) C17B—C16B—H16B 120.1
C15A—C14A—O3A 124.6 (4) C18B—C17B—C16B 118.9 (5)
C15A—C14A—C13A 121.4 (4) C18B—C17B—H17B 120.5
O3A—C14A—C13A 114.0 (3) C16B—C17B—H17B 120.5
C16A—C15A—C14A 119.5 (5) C13B—C18B—C17B 122.5 (4)
C16A—C15A—H15A 120.3 C13B—C18B—H18B 118.8
C14A—C15A—H15A 120.3 C17B—C18B—H18B 118.8
C15A—C16A—C17A 124.1 (4) O1B—C19B—H19D 109.5
C15A—C16A—H16A 117.9 O1B—C19B—H19E 109.5
C17A—C16A—H16A 117.9 H19D—C19B—H19E 109.5
C16A—C17A—C18A 112.7 (5) O1B—C19B—H19F 109.5
C16A—C17A—H17A 123.7 H19D—C19B—H19F 109.5
C18A—C17A—H17A 123.7 H19E—C19B—H19F 109.5
C13A—C18A—C17A 125.3 (4) O2B—C20B—H20D 109.5
C13A—C18A—H18A 117.4 O2B—C20B—H20E 109.5
C17A—C18A—H18A 117.4 H20D—C20B—H20E 109.5
C1B—P1B—C7B 100.11 (12) O2B—C20B—H20F 109.5
C1B—P1B—C13B 100.60 (10) H20D—C20B—H20F 109.5
C7B—P1B—C13B 101.19 (14) H20E—C20B—H20F 109.5
C2B—O1B—C19B 118.9 (2) O3B—C21B—H21D 109.5
C8B—O2B—C20B 116.4 (3) O3B—C21B—H21E 109.5
C14B—O3B—C21B 113.3 (3) H21D—C21B—H21E 109.5
C2B—C1B—C6B 116.71 (16) O3B—C21B—H21F 109.5
C2B—C1B—P1B 118.9 H21D—C21B—H21F 109.5
C6B—C1B—P1B 124.34 (16) H21E—C21B—H21F 109.5
C13A—P1A—C1A—C2A 87.8 (3) C7B—P1B—C1B—C2B 85.86 (10)
C7A—P1A—C1A—C2A −167.3 (3) C13B—P1B—C1B—C2B −170.61 (10)
C13A—P1A—C1A—C6A −96.6 (3) C7B—P1B—C1B—C6B −93.9 (2)
C7A—P1A—C1A—C6A 8.4 (3) C13B—P1B—C1B—C6B 9.6 (3)
C19A—O1A—C2A—C1A 161.8 (4) C19B—O1B—C2B—C3B −9.9 (3)
C19A—O1A—C2A—C3A −17.4 (7) C19B—O1B—C2B—C1B 171.4 (3)
C6A—C1A—C2A—O1A 178.4 (4) C6B—C1B—C2B—O1B 176.5 (2)
P1A—C1A—C2A—O1A −5.7 (5) P1B—C1B—C2B—O1B −3.3
C6A—C1A—C2A—C3A −2.3 (5) C6B—C1B—C2B—C3B −2.20 (18)
P1A—C1A—C2A—C3A 173.6 (3) P1B—C1B—C2B—C3B 177.99 (8)
O1A—C2A—C3A—C4A −178.6 (5) O1B—C2B—C3B—C4B −174.7 (2)
C1A—C2A—C3A—C4A 2.2 (6) C1B—C2B—C3B—C4B 3.85 (19)
C2A—C3A—C4A—C5A 0.7 (8) C2B—C3B—C4B—C5B −3.6 (6)
C3A—C4A—C5A—C6A −3.5 (10) C3B—C4B—C5B—C6B 1.9 (10)
C4A—C5A—C6A—C1A 3.3 (9) C4B—C5B—C6B—C1B −0.3 (10)
C2A—C1A—C6A—C5A −0.4 (6) C2B—C1B—C6B—C5B 0.5 (6)
P1A—C1A—C6A—C5A −176.1 (5) P1B—C1B—C6B—C5B −179.7 (5)
C13A—P1A—C7A—C8A −179.0 (3) C1B—P1B—C7B—C12B −4.2 (3)
C1A—P1A—C7A—C8A 76.4 (3) C13B—P1B—C7B—C12B −107.2 (3)
C13A—P1A—C7A—C12A −6.2 (3) C1B—P1B—C7B—C8B 178.8 (2)
C1A—P1A—C7A—C12A −110.8 (3) C13B—P1B—C7B—C8B 75.8 (3)
C20A—O2A—C8A—C9A −2.4 (7) C20B—O2B—C8B—C9B 4.0 (5)
C20A—O2A—C8A—C7A 177.0 (4) C20B—O2B—C8B—C7B −175.1 (3)
C12A—C7A—C8A—O2A −179.4 (3) C12B—C7B—C8B—C9B 1.7 (5)
P1A—C7A—C8A—O2A −6.1 (5) P1B—C7B—C8B—C9B 178.9 (3)
C12A—C7A—C8A—C9A −0.1 (6) C12B—C7B—C8B—O2B −179.2 (3)
P1A—C7A—C8A—C9A 173.3 (4) P1B—C7B—C8B—O2B −2.0 (3)
O2A—C8A—C9A—C10A 179.2 (5) O2B—C8B—C9B—C10B 179.8 (3)
C7A—C8A—C9A—C10A −0.1 (8) C7B—C8B—C9B—C10B −1.2 (6)
C8A—C9A—C10A—C11A 0.1 (8) C8B—C9B—C10B—C11B 2.2 (7)
C9A—C10A—C11A—C12A 0.1 (7) C9B—C10B—C11B—C12B −3.7 (8)
C8A—C7A—C12A—C11A 0.3 (5) C10B—C11B—C12B—C7B 4.4 (8)
P1A—C7A—C12A—C11A −172.5 (3) C8B—C7B—C12B—C11B −3.6 (6)
C10A—C11A—C12A—C7A −0.3 (6) P1B—C7B—C12B—C11B 179.4 (4)
C7A—P1A—C13A—C18A −107.9 (3) C1B—P1B—C13B—C18B −104.3 (3)
C1A—P1A—C13A—C18A −3.4 (4) C7B—P1B—C13B—C18B −1.7 (3)
C7A—P1A—C13A—C14A 79.2 (3) C1B—P1B—C13B—C14B 78.1 (3)
C1A—P1A—C13A—C14A −176.3 (3) C7B—P1B—C13B—C14B −179.2 (3)
C21A—O3A—C14A—C15A −6.9 (7) C21B—O3B—C14B—C15B −2.0 (7)
C21A—O3A—C14A—C13A 173.7 (3) C21B—O3B—C14B—C13B 178.4 (5)
C18A—C13A—C14A—C15A 2.3 (7) C18B—C13B—C14B—O3B 178.4 (3)
P1A—C13A—C14A—C15A 175.8 (5) P1B—C13B—C14B—O3B −3.9 (4)
C18A—C13A—C14A—O3A −178.2 (4) C18B—C13B—C14B—C15B −1.2 (6)
P1A—C13A—C14A—O3A −4.8 (5) P1B—C13B—C14B—C15B 176.5 (4)
O3A—C14A—C15A—C16A 178.4 (5) O3B—C14B—C15B—C16B −177.9 (5)
C13A—C14A—C15A—C16A −2.2 (9) C13B—C14B—C15B—C16B 1.6 (8)
C14A—C15A—C16A—C17A 3.6 (11) C14B—C15B—C16B—C17B −1.7 (9)
C15A—C16A—C17A—C18A −4.8 (10) C15B—C16B—C17B—C18B 1.4 (8)
C14A—C13A—C18A—C17A −4.1 (7) C14B—C13B—C18B—C17B 0.9 (6)
P1A—C13A—C18A—C17A −177.1 (5) P1B—C13B—C18B—C17B −176.7 (4)
C16A—C17A—C18A—C13A 5.1 (9) C16B—C17B—C18B—C13B −1.0 (7)