| Bruker APEXII CCD area-detector diffractometer | 3162 independent reflections |
| Radiation source: fine-focus sealed tube | 2371 reflections with I > 2σ(I) |
| graphite | Rint = 0.082 |
| φ and ω scans | θmax = 25.0°, θmin = 3.0° |
| Absorption correction: multi-scan (SADABS; Bruker, 2004) | h = −27→29 |
| Tmin = 0.914, Tmax = 0.941 | k = −13→13 |
| 11927 measured reflections | l = −14→13 |