| Rigaku R-AXIS RAPID IP diffractometer | 3833 independent reflections |
| Radiation source: fine-focus sealed tube | 2302 reflections with I > 2σ(I) |
| graphite | Rint = 0.046 |
| Detector resolution: 10.00 pixels mm-1 | θmax = 27.5°, θmin = 2.1° |
| Ω scans | h = −17→17 |
| Absorption correction: multi-scan (ABSCOR; Higashi,1995) | k = −11→11 |
| Tmin = 0.944, Tmax = 0.972 | l = −18→18 |
| 15335 measured reflections |
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