Br1—C3 | 1.896 (2) | C3—C4 | 1.390 (3) |
Ni1—O1i | 2.0806 (16) | C4—C5 | 1.383 (4) |
Ni1—O1 | 2.0806 (16) | C4—H4 | 0.9300 |
Ni1—O4 | 2.1012 (17) | C5—C6 | 1.382 (4) |
Ni1—O4i | 2.1012 (17) | C5—H5 | 0.9300 |
Ni1—N1 | 2.068 (2) | C6—C7 | 1.390 (3) |
Ni1—N1i | 2.068 (2) | C6—H6 | 0.9300 |
O1—C1 | 1.260 (3) | C7—H7 | 0.9300 |
O2—C1 | 1.258 (3) | C8—H8 | 0.9300 |
O3—C13 | 1.241 (3) | C9—C8 | 1.377 (3) |
O4—H41 | 0.86 (4) | C9—H9 | 0.9300 |
O4—H42 | 0.83 (4) | C10—C9 | 1.391 (3) |
N1—C8 | 1.347 (3) | C10—H10 | 0.9300 |
N1—C12 | 1.337 (3) | C11—C10 | 1.383 (3) |
N2—H21 | 0.82 (4) | C11—C12 | 1.390 (3) |
N2—H22 | 0.79 (4) | C12—H12 | 0.9300 |
C1—C2 | 1.513 (3) | C13—N2 | 1.327 (3) |
C2—C7 | 1.394 (3) | C13—C11 | 1.505 (3) |
C3—C2 | 1.400 (4) | ||
O1i—Ni1—O1 | 180.000 (1) | C4—C3—Br1 | 115.24 (18) |
O1—Ni1—O4 | 87.40 (7) | C4—C3—C2 | 121.6 (2) |
O1i—Ni1—O4 | 92.60 (7) | C3—C4—H4 | 120.2 |
O1i—Ni1—O4i | 87.40 (7) | C5—C4—C3 | 119.7 (2) |
O1—Ni1—O4i | 92.60 (7) | C5—C4—H4 | 120.2 |
O4—Ni1—O4i | 180.00 (10) | C4—C5—H5 | 119.9 |
N1—Ni1—O1 | 89.60 (7) | C6—C5—C4 | 120.2 (2) |
N1i—Ni1—O1 | 90.40 (7) | C6—C5—H5 | 119.9 |
N1—Ni1—O1i | 90.40 (7) | C5—C6—C7 | 119.5 (2) |
N1i—Ni1—O1i | 89.60 (7) | C5—C6—H6 | 120.3 |
N1—Ni1—O4 | 87.68 (7) | C7—C6—H6 | 120.3 |
N1i—Ni1—O4 | 92.32 (7) | C2—C7—H7 | 119.0 |
N1—Ni1—O4i | 92.32 (7) | C6—C7—C2 | 122.0 (2) |
N1i—Ni1—O4i | 87.68 (7) | C6—C7—H7 | 119.0 |
N1—Ni1—N1i | 180.00 (10) | N1—C8—C9 | 123.0 (2) |
C1—O1—Ni1 | 122.99 (15) | N1—C8—H8 | 118.5 |
Ni1—O4—H41 | 95 (3) | C9—C8—H8 | 118.5 |
Ni1—O4—H42 | 124 (2) | C8—C9—C10 | 118.8 (2) |
H42—O4—H41 | 105 (4) | C8—C9—H9 | 120.6 |
C8—N1—Ni1 | 122.66 (15) | C10—C9—H9 | 120.6 |
C12—N1—Ni1 | 119.53 (16) | C9—C10—H10 | 120.6 |
C12—N1—C8 | 117.8 (2) | C11—C10—C9 | 118.8 (2) |
C13—N2—H21 | 121 (3) | C11—C10—H10 | 120.6 |
C13—N2—H22 | 118 (2) | C10—C11—C12 | 118.7 (2) |
H21—N2—H22 | 118 (3) | C10—C11—C13 | 124.0 (2) |
O1—C1—C2 | 117.8 (2) | C12—C11—C13 | 117.3 (2) |
O2—C1—O1 | 124.7 (2) | N1—C12—C11 | 123.0 (2) |
O2—C1—C2 | 117.4 (2) | N1—C12—H12 | 118.5 |
C3—C2—C1 | 124.1 (2) | C11—C12—H12 | 118.5 |
C7—C2—C1 | 118.8 (2) | O3—C13—N2 | 122.8 (2) |
C7—C2—C3 | 117.0 (2) | O3—C13—C11 | 119.9 (2) |
C2—C3—Br1 | 123.11 (17) | N2—C13—C11 | 117.2 (2) |
O4—Ni1—O1—C1 | −145.89 (18) | C1—C2—C7—C6 | −172.5 (2) |
O4i—Ni1—O1—C1 | 34.11 (18) | C3—C2—C7—C6 | 2.3 (4) |
N1—Ni1—O1—C1 | −58.20 (18) | Br1—C3—C2—C1 | −10.9 (3) |
N1i—Ni1—O1—C1 | 121.80 (18) | Br1—C3—C2—C7 | 174.53 (17) |
O1—Ni1—N1—C8 | 137.00 (19) | C4—C3—C2—C1 | 171.3 (2) |
O1i—Ni1—N1—C8 | −43.00 (19) | C4—C3—C2—C7 | −3.2 (4) |
O1—Ni1—N1—C12 | −44.08 (18) | Br1—C3—C4—C5 | −176.67 (19) |
O1i—Ni1—N1—C12 | 135.92 (18) | C2—C3—C4—C5 | 1.2 (4) |
O4—Ni1—N1—C12 | 43.33 (18) | C3—C4—C5—C6 | 1.7 (4) |
O4i—Ni1—N1—C12 | −136.67 (18) | C4—C5—C6—C7 | −2.6 (4) |
O4—Ni1—N1—C8 | −135.59 (19) | C5—C6—C7—C2 | 0.5 (4) |
O4i—Ni1—N1—C8 | 44.41 (19) | C10—C9—C8—N1 | 0.7 (4) |
Ni1—O1—C1—O2 | −19.9 (3) | C11—C10—C9—C8 | 0.2 (4) |
Ni1—O1—C1—C2 | 155.74 (16) | C12—C11—C10—C9 | −0.9 (4) |
Ni1—N1—C8—C9 | 178.11 (19) | C13—C11—C10—C9 | 176.4 (2) |
C12—N1—C8—C9 | −0.8 (4) | C10—C11—C12—N1 | 0.8 (4) |
Ni1—N1—C12—C11 | −178.89 (18) | C13—C11—C12—N1 | −176.7 (2) |
C8—N1—C12—C11 | 0.1 (4) | O3—C13—C11—C10 | −173.8 (2) |
O1—C1—C2—C3 | 156.0 (2) | O3—C13—C11—C12 | 3.5 (4) |
O1—C1—C2—C7 | −29.6 (3) | N2—C13—C11—C10 | 4.7 (4) |
O2—C1—C2—C3 | −28.0 (4) | N2—C13—C11—C12 | −178.0 (2) |
O2—C1—C2—C7 | 146.4 (2) |