| C1—C22 | 1.208 (16) | C5—O6 | 1.186 (3) |
| C1—C21 | 1.265 (5) | C5—O7 | 1.335 (3) |
| C1—H1A | 0.9300 | O7—C8 | 1.418 (2) |
| C1—H1B | 0.9300 | C8—C13 | 1.362 (4) |
| C1—H1C | 0.9300 | C8—C9 | 1.379 (3) |
| C1—H1D | 0.9300 | C9—C10 | 1.371 (3) |
| C21—C3 | 1.482 (4) | C9—H9A | 0.9300 |
| C21—H21A | 0.9300 | C10—C11 | 1.392 (3) |
| C22—C3 | 1.414 (13) | C10—H10A | 0.9300 |
| C22—H22A | 0.9300 | C11—O14 | 1.362 (2) |
| C3—O4 | 1.454 (4) | C11—C12 | 1.387 (3) |
| C3—H3A | 0.9700 | C12—C13 | 1.388 (3) |
| C3—H3B | 0.9700 | C12—H12A | 0.9300 |
| C3—H3C | 0.9700 | C13—H13A | 0.9300 |
| C3—H3D | 0.9700 | O14—H14 | 0.8830 |
| O4—C5 | 1.315 (3) | ||
| H1A—C1—H1B | 120.0 | C5—O4—C3 | 114.8 (2) |
| H1C—C1—H1D | 120.0 | O6—C5—O4 | 126.6 (2) |
| C21—C1—H1A | 120.0 | O6—C5—O7 | 125.9 (2) |
| C21—C1—H1B | 120.0 | O4—C5—O7 | 107.52 (19) |
| C22—C1—H1C | 126.5 | C5—O7—C8 | 117.36 (17) |
| C22—C1—H1D | 113.2 | C13—C8—C9 | 121.3 (2) |
| C1—C21—C3 | 124.7 (4) | C13—C8—O7 | 118.65 (19) |
| C1—C22—C3 | 136.4 (14) | C9—C8—O7 | 119.9 (2) |
| C1—C21—H21A | 117.7 | C10—C9—C8 | 119.7 (2) |
| C1—C22—H22A | 111.8 | C10—C9—H9A | 120.1 |
| C3—C21—H21A | 117.7 | C8—C9—H9A | 120.1 |
| C3—C22—H22A | 111.8 | C9—C10—C11 | 119.77 (19) |
| C22—C3—O4 | 112.2 (8) | C9—C10—H10A | 120.1 |
| O4—C3—C21 | 107.5 (3) | C11—C10—H10A | 120.1 |
| O4—C3—H3A | 110.2 | O14—C11—C12 | 117.2 (2) |
| O4—C3—H3B | 110.2 | O14—C11—C10 | 122.85 (18) |
| C21—C3—H3A | 110.2 | C12—C11—C10 | 119.95 (19) |
| C21—C3—H3B | 110.2 | C11—C12—C13 | 119.6 (2) |
| H3A—C3—H3B | 108.5 | C11—C12—H12A | 120.2 |
| C22—C3—H3C | 110.8 | C13—C12—H12A | 120.2 |
| C22—C3—H3D | 109.2 | C8—C13—C12 | 119.64 (19) |
| O4—C3—H3C | 108.3 | C8—C13—H13A | 120.2 |
| O4—C3—H3D | 108.8 | C12—C13—H13A | 120.2 |
| C21—C3—H3C | 142.5 | C11—O14—H14 | 111.4 |
| H3C—C3—H3D | 107.5 | ||
| C22—C1—C21—C3 | −15.6 (12) | C5—O7—C8—C13 | 87.7 (3) |
| C21—C1—C22—C3 | 19.6 (16) | C5—O7—C8—C9 | −97.1 (3) |
| C1—C22—C3—O4 | −111 (2) | C13—C8—C9—C10 | 1.0 (4) |
| C1—C22—C3—C21 | −19.0 (16) | O7—C8—C9—C10 | −174.1 (2) |
| C1—C21—C3—C22 | 15.1 (11) | C8—C9—C10—C11 | 0.3 (3) |
| C1—C21—C3—O4 | 119.1 (4) | C9—C10—C11—O14 | 179.3 (2) |
| C22—C3—O4—C5 | −128.5 (9) | C9—C10—C11—C12 | −1.6 (3) |
| C21—C3—O4—C5 | −174.7 (3) | O14—C11—C12—C13 | −179.3 (2) |
| C3—O4—C5—O6 | −2.4 (4) | C10—C11—C12—C13 | 1.5 (4) |
| C3—O4—C5—O7 | 176.2 (3) | C9—C8—C13—C12 | −1.1 (4) |
| O6—C5—O7—C8 | 3.8 (4) | O7—C8—C13—C12 | 174.0 (2) |
| O4—C5—O7—C8 | −174.8 (2) | C11—C12—C13—C8 | −0.1 (4) |