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. 2009 Jun 10;65(Pt 7):o1541–o1542. doi: 10.1107/S160053680902131X
O1A—C8A 1.2463 (15) O1B—C8B 1.2395 (16)
O2A—C10A 1.2123 (15) O2B—C10B 1.2120 (15)
O3A—C10A 1.3419 (16) O3B—C10B 1.3413 (16)
O3A—C11A 1.4514 (14) O3B—C11B 1.4542 (15)
N1A—N2A 1.3040 (14) N1B—N2B 1.3033 (14)
N1A—C6A 1.4132 (16) N1B—C6B 1.4125 (15)
N1A—H1NA 0.904 (18) N1B—H1NB 0.91 (2)
N2A—C7A 1.3287 (16) N2B—C7B 1.3287 (16)
C1A—C2A 1.3905 (18) C1B—C2B 1.3914 (18)
C1A—C6A 1.4126 (17) C1B—C6B 1.4121 (17)
C1A—C13A 1.5095 (19) C1B—C13B 1.5069 (19)
C2A—C3A 1.385 (2) C2B—C3B 1.382 (2)
C2A—H2AA 0.930 C2B—H2BA 0.930
C3A—C4A 1.3845 (19) C3B—C4B 1.3874 (18)
C3A—H3AA 0.930 C3B—H3BA 0.930
C4A—C5A 1.3979 (18) C4B—C5B 1.3985 (17)
C4A—H4AA 0.930 C4B—H4BA 0.930
C5A—C6A 1.4060 (18) C5B—C6B 1.4095 (18)
C5A—C14A 1.5112 (17) C5B—C14B 1.5076 (17)
C7A—C8A 1.4690 (18) C7B—C8B 1.4702 (18)
C7A—C10A 1.4876 (17) C7B—C10B 1.4864 (17)
C8A—C9A 1.4953 (18) C8B—C9B 1.4994 (18)
C9A—H9AA 0.960 C9B—H9BA 0.960
C9A—H9AB 0.960 C9B—H9BB 0.960
C9A—H9AC 0.960 C9B—H9BC 0.960
C11A—C12A 1.5075 (18) C11B—C12B 1.5046 (19)
C11A—H11A 0.970 C11B—H11C 0.970
C11A—H11B 0.970 C11B—H11D 0.970
C12A—H12A 0.960 C12B—H12D 0.960
C12A—H12B 0.960 C12B—H12E 0.960
C12A—H12C 0.960 C12B—H12F 0.960
C13A—H13A 0.960 C13B—H13D 0.960
C13A—H13B 0.960 C13B—H13E 0.960
C13A—H13C 0.960 C13B—H13F 0.960
C14A—H14A 0.960 C14B—H14D 0.960
C14A—H14B 0.960 C14B—H14E 0.960
C14A—H14C 0.960 C14B—H14F 0.960
C10A—O3A—C11A 115.28 (9) C10B—O3B—C11B 115.88 (10)
N2A—N1A—C6A 123.25 (11) N2B—N1B—C6B 122.54 (11)
N2A—N1A—H1NA 116.5 (11) N2B—N1B—H1NB 116.9 (12)
C6A—N1A—H1NA 120.3 (11) C6B—N1B—H1NB 120.5 (12)
N1A—N2A—C7A 119.54 (11) N1B—N2B—C7B 120.63 (11)
C2A—C1A—C6A 118.63 (13) C2B—C1B—C6B 118.34 (12)
C2A—C1A—C13A 120.51 (12) C2B—C1B—C13B 120.25 (12)
C6A—C1A—C13A 120.86 (12) C6B—C1B—C13B 121.42 (12)
C3A—C2A—C1A 120.60 (13) C3B—C2B—C1B 121.15 (12)
C3A—C2A—H2AA 119.7 C3B—C2B—H2BA 119.4
C1A—C2A—H2AA 119.7 C1B—C2B—H2BA 119.4
C4A—C3A—C2A 119.87 (12) C2B—C3B—C4B 119.61 (12)
C4A—C3A—H3AA 120.1 C2B—C3B—H3BA 120.2
C2A—C3A—H3AA 120.1 C4B—C3B—H3BA 120.2
C3A—C4A—C5A 122.25 (13) C3B—C4B—C5B 122.15 (12)
C3A—C4A—H4AA 118.9 C3B—C4B—H4BA 118.9
C5A—C4A—H4AA 118.9 C5B—C4B—H4BA 118.9
C4A—C5A—C6A 116.83 (12) C4B—C5B—C6B 116.98 (11)
C4A—C5A—C14A 118.80 (12) C4B—C5B—C14B 118.48 (11)
C6A—C5A—C14A 124.37 (11) C6B—C5B—C14B 124.54 (11)
C5A—C6A—C1A 121.81 (11) C5B—C6B—C1B 121.76 (11)
C5A—C6A—N1A 124.07 (11) C5B—C6B—N1B 123.48 (11)
C1A—C6A—N1A 114.11 (12) C1B—C6B—N1B 114.76 (11)
N2A—C7A—C8A 124.19 (11) N2B—C7B—C8B 123.97 (11)
N2A—C7A—C10A 113.99 (11) N2B—C7B—C10B 113.80 (11)
C8A—C7A—C10A 121.82 (11) C8B—C7B—C10B 122.23 (11)
O1A—C8A—C7A 119.14 (11) O1B—C8B—C7B 118.96 (11)
O1A—C8A—C9A 118.76 (12) O1B—C8B—C9B 119.06 (12)
C7A—C8A—C9A 122.09 (11) C7B—C8B—C9B 121.98 (12)
C8A—C9A—H9AA 109.5 C8B—C9B—H9BA 109.5
C8A—C9A—H9AB 109.5 C8B—C9B—H9BB 109.5
H9AA—C9A—H9AB 109.5 H9BA—C9B—H9BB 109.5
C8A—C9A—H9AC 109.5 C8B—C9B—H9BC 109.5
H9AA—C9A—H9AC 109.5 H9BA—C9B—H9BC 109.5
H9AB—C9A—H9AC 109.5 H9BB—C9B—H9BC 109.5
O2A—C10A—O3A 122.70 (11) O2B—C10B—O3B 122.89 (12)
O2A—C10A—C7A 125.05 (12) O2B—C10B—C7B 124.62 (12)
O3A—C10A—C7A 112.25 (10) O3B—C10B—C7B 112.48 (10)
O3A—C11A—C12A 106.82 (10) O3B—C11B—C12B 106.66 (10)
O3A—C11A—H11A 110.4 O3B—C11B—H11C 110.4
C12A—C11A—H11A 110.4 C12B—C11B—H11C 110.4
O3A—C11A—H11B 110.4 O3B—C11B—H11D 110.4
C12A—C11A—H11B 110.4 C12B—C11B—H11D 110.4
H11A—C11A—H11B 108.6 H11C—C11B—H11D 108.6
C11A—C12A—H12A 109.5 C11B—C12B—H12D 109.5
C11A—C12A—H12B 109.5 C11B—C12B—H12E 109.5
H12A—C12A—H12B 109.5 H12D—C12B—H12E 109.5
C11A—C12A—H12C 109.5 C11B—C12B—H12F 109.5
H12A—C12A—H12C 109.5 H12D—C12B—H12F 109.5
H12B—C12A—H12C 109.5 H12E—C12B—H12F 109.5
C1A—C13A—H13A 109.5 C1B—C13B—H13D 109.5
C1A—C13A—H13B 109.5 C1B—C13B—H13E 109.5
H13A—C13A—H13B 109.5 H13D—C13B—H13E 109.5
C1A—C13A—H13C 109.5 C1B—C13B—H13F 109.5
H13A—C13A—H13C 109.5 H13D—C13B—H13F 109.5
H13B—C13A—H13C 109.5 H13E—C13B—H13F 109.5
C5A—C14A—H14A 109.5 C5B—C14B—H14D 109.5
C5A—C14A—H14B 109.5 C5B—C14B—H14E 109.5
H14A—C14A—H14B 109.5 H14D—C14B—H14E 109.5
C5A—C14A—H14C 109.5 C5B—C14B—H14F 109.5
H14A—C14A—H14C 109.5 H14D—C14B—H14F 109.5
H14B—C14A—H14C 109.5 H14E—C14B—H14F 109.5
C6A—N1A—N2A—C7A 179.03 (12) C6B—N1B—N2B—C7B −179.54 (12)
C6A—C1A—C2A—C3A −0.2 (2) C6B—C1B—C2B—C3B −0.2 (2)
C13A—C1A—C2A—C3A 179.61 (14) C13B—C1B—C2B—C3B 179.80 (14)
C1A—C2A—C3A—C4A 1.1 (2) C1B—C2B—C3B—C4B −0.2 (2)
C2A—C3A—C4A—C5A −0.8 (2) C2B—C3B—C4B—C5B 0.1 (2)
C3A—C4A—C5A—C6A −0.3 (2) C3B—C4B—C5B—C6B 0.3 (2)
C3A—C4A—C5A—C14A 179.28 (13) C3B—C4B—C5B—C14B −179.27 (13)
C4A—C5A—C6A—C1A 1.2 (2) C4B—C5B—C6B—C1B −0.78 (19)
C14A—C5A—C6A—C1A −178.33 (13) C14B—C5B—C6B—C1B 178.79 (13)
C4A—C5A—C6A—N1A −178.53 (12) C4B—C5B—C6B—N1B 179.62 (12)
C14A—C5A—C6A—N1A 1.9 (2) C14B—C5B—C6B—N1B −0.8 (2)
C2A—C1A—C6A—C5A −1.0 (2) C2B—C1B—C6B—C5B 0.7 (2)
C13A—C1A—C6A—C5A 179.22 (13) C13B—C1B—C6B—C5B −179.29 (13)
C2A—C1A—C6A—N1A 178.77 (12) C2B—C1B—C6B—N1B −179.62 (12)
C13A—C1A—C6A—N1A −1.02 (19) C13B—C1B—C6B—N1B 0.34 (19)
N2A—N1A—C6A—C5A 2.0 (2) N2B—N1B—C6B—C5B −2.4 (2)
N2A—N1A—C6A—C1A −177.74 (12) N2B—N1B—C6B—C1B 178.02 (12)
N1A—N2A—C7A—C8A −0.6 (2) N1B—N2B—C7B—C8B 0.9 (2)
N1A—N2A—C7A—C10A 179.99 (11) N1B—N2B—C7B—C10B −179.37 (11)
N2A—C7A—C8A—O1A −0.6 (2) N2B—C7B—C8B—O1B −1.9 (2)
C10A—C7A—C8A—O1A 178.82 (13) C10B—C7B—C8B—O1B 178.34 (13)
N2A—C7A—C8A—C9A −179.80 (13) N2B—C7B—C8B—C9B 177.42 (13)
C10A—C7A—C8A—C9A −0.4 (2) C10B—C7B—C8B—C9B −2.3 (2)
C11A—O3A—C10A—O2A 0.89 (19) C11B—O3B—C10B—O2B −1.24 (19)
C11A—O3A—C10A—C7A −178.87 (11) C11B—O3B—C10B—C7B 178.20 (11)
N2A—C7A—C10A—O2A 178.94 (13) N2B—C7B—C10B—O2B 178.42 (13)
C8A—C7A—C10A—O2A −0.5 (2) C8B—C7B—C10B—O2B −1.8 (2)
N2A—C7A—C10A—O3A −1.31 (16) N2B—C7B—C10B—O3B −1.00 (17)
C8A—C7A—C10A—O3A 179.24 (12) C8B—C7B—C10B—O3B 178.78 (12)
C10A—O3A—C11A—C12A 179.37 (11) C10B—O3B—C11B—C12B −177.50 (11)