Bruker SMART APEXII CCD diffractometer | 6206 independent reflections |
Radiation source: fine-focus sealed tube | 4862 reflections with I > 2σ(I) |
graphite | Rint = 0.037 |
φ and ω scans | θmax = 27.5°, θmin = 2.1° |
Absorption correction: multi-scan (SADABS; Bruker, 2005) | h = −8→8 |
Tmin = 0.962, Tmax = 0.991 | k = −22→22 |
38064 measured reflections | l = −29→29 |