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. 2009 May 20;65(Pt 6):o1347. doi: 10.1107/S1600536809018303
Refinement on F2 Primary atom site location: structure-invariant direct methods
Least-squares matrix: full Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.063 Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.138 H-atom parameters constrained
S = 0.91 w = 1/[σ2(Fo2) + (0.0441P)2] where P = (Fo2 + 2Fc2)/3
2613 reflections (Δ/σ)max < 0.001
183 parameters Δρmax = 0.28 e Å3
0 restraints Δρmin = −0.27 e Å3