Refinement on F2	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.052	Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.140	H atoms treated by a mixture of independent and constrained refinement
S = 1.01	w = 1/[σ2(Fo2) + (0.0657P)2 + 0.3754P] where P = (Fo2 + 2Fc2)/3
3236 reflections	(Δ/σ)max = 0.001
187 parameters	Δρmax = 0.38 e Å−3
1 restraint	Δρmin = −0.25 e Å−3