| Rigaku Mercury diffractometer | 3349 independent reflections |
| Radiation source: fine-focus sealed tube | 2614 reflections with I > 2/s(I) |
| graphite | Rint = 0.027 |
| Detector resolution: 7.31 pixels mm-1 | θmax = 25.3°, θmin = 3.1° |
| ω scans | h = −11→11 |
| Absorption correction: multi-scan (ABSCOR; Jacobson, 1998) | k = −10→11 |
| Tmin = 0.966, Tmax = 0.976 | l = −13→13 |
| 8987 measured reflections |
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