| Bruker SMART 1000 CCD diffractometer | 3237 independent reflections |
| Radiation source: fine-focus sealed tube | 2940 reflections with I > 2σ(I) |
| graphite | Rint = 0.017 |
| ω scans | θmax = 26.0°, θmin = 2.0° |
| Absorption correction: multi-scan (SADABS; Bruker, 2004) | h = −11→11 |
| Tmin = 0.370, Tmax = 0.594 | k = −11→11 |
| 6537 measured reflections | l = −14→11 |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.