| Bruker SMART CCD area-detector diffractometer | 1099 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.024 |
| graphite | θmax = 26.0°, θmin = 2.4° |
| ω scans | h = −9→8 |
| 7304 measured reflections | k = −11→12 |
| 2116 independent reflections | l = −13→18 |
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