Bruker APEXII CCD diffractometer | 1377 independent reflections |
Radiation source: fine-focus sealed tube | 1270 reflections with I > 2σ(I) |
graphite | Rint = 0.030 |
φ and ω scans | θmax = 25.0°, θmin = 3.4° |
Absorption correction: multi-scan (SADABS; Bruker, 2004) | h = −8→8 |
Tmin = 0.987, Tmax = 0.991 | k = −11→13 |
6725 measured reflections | l = −33→40 |