| Bruker SMART APEX CCD diffractometer | 2741 independent reflections |
| Radiation source: fine-focus sealed tube | 2512 reflections with I > 2σ(I) |
| graphite | Rint = 0.026 |
| φ and ω scans | θmax = 27.0°, θmin = 2.5° |
| Absorption correction: multi-scan (SADABS; Bruker, 1997) | h = −21→21 |
| Tmin = 0.692, Tmax = 0.834 | k = −6→11 |
| 7147 measured reflections | l = −21→21 |