Bruker–Nonius KappaCCD diffractometer | 1046 reflections with I > 2σ(I) |
Radiation source: fine-focus sealed tube | Rint = 0.064 |
φ and ω scans | θmax = 27.5°, θmin = 4.7° |
Absorption correction: numerical HABITUS (Herrendorf & Bärnighausen, 1997) | h = −9→9 |
Tmin = 0.325, Tmax = 0.455 | k = −6→6 |
8638 measured reflections | l = −17→22 |
1420 independent reflections |