Bruker Kappa APEXII CCD diffractometer | 4226 independent reflections |
Radiation source: fine-focus sealed tube | 3259 reflections with I > 2σ(I) |
graphite | Rint = 0.025 |
ω scans | θmax = 30.2°, θmin = 1.7° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −6→11 |
Tmin = 0.978, Tmax = 0.982 | k = −11→12 |
19570 measured reflections | l = −17→17 |