| Bruker APEXII CCD diffractometer | 3772 independent reflections |
| Radiation source: fine-focus sealed tube | 2737 reflections with I > 2σ(I) |
| graphite | Rint = 0.072 |
| φ and ω scans | θmax = 24.7°, θmin = 1.9° |
| Absorption correction: multi-scan (SADABS; Bruker, 1997) | h = −11→11 |
| Tmin = 0.957, Tmax = 0.993 | k = −12→12 |
| 20692 measured reflections | l = −25→24 |