| Bruker SMART CCD area-detector diffractometer | 2204 independent reflections |
| Radiation source: fine-focus sealed tube | 2029 reflections with I > 2σ(I) |
| graphite | Rint = 0.019 |
| φ and ω scans | θmax = 25.2°, θmin = 2.0° |
| Absorption correction: multi-scan (Jacobson, 1998) | h = −8→8 |
| Tmin = 0.901, Tmax = 0.950 | k = −10→10 |
| 8018 measured reflections | l = −12→11 |