| Rigaku/MSC Mercury CCD diffractometer | 1323 reflections with I > 2σ(I) |
| Radiation source: Rotating Anode | Rint = 0.044 |
| Graphite Monochromator | θmax = 30.8°, θmin = 3.7° |
| Detector resolution: 14.62 pixels mm-1 | h = −9→9 |
| φ and ω scans | k = −9→5 |
| 2656 measured reflections | l = −7→10 |
| 1661 independent reflections |
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