Bruker APEXII area-detector diffractometer | 4741 independent reflections |
Radiation source: fine-focus sealed tube | 4175 reflections with I > 2σ(I) |
graphite | Rint = 0.021 |
φ and ω scans | θmax = 25.0°, θmin = 1.8° |
Absorption correction: multi-scan (SADABS; Bruker, 2004) | h = −11→11 |
Tmin = 0.501, Tmax = 0.592 | k = −15→16 |
16112 measured reflections | l = −23→23 |