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. 2009 Sep 5;65(Pt 10):o2330. doi: 10.1107/S1600536809033418
Enraf–Nonius KappaCCD diffractometer 1485 reflections with I > 2σ(I)
Radiation source: fine-focus sealed tube Rint = 0.018
graphite θmax = 27.5°, θmin = 6.4°
Detector resolution: 9 pixels mm-1 h = −9→9
φ and ω scans k = −16→15
4410 measured reflections l = −10→10
1678 independent reflections