Enraf–Nonius KappaCCD diffractometer | 1485 reflections with I > 2σ(I) |
Radiation source: fine-focus sealed tube | Rint = 0.018 |
graphite | θmax = 27.5°, θmin = 6.4° |
Detector resolution: 9 pixels mm-1 | h = −9→9 |
φ and ω scans | k = −16→15 |
4410 measured reflections | l = −10→10 |
1678 independent reflections |