Refinement on F2 | Primary atom site location: structure-invariant direct methods |
Least-squares matrix: full | Secondary atom site location: difference Fourier map |
R[F2 > 2σ(F2)] = 0.038 | Hydrogen site location: difference Fourier map |
wR(F2) = 0.095 | H atoms treated by a mixture of independent and constrained refinement |
S = 1.04 | w = 1/[σ2(Fo2) + (0.0482P)2 + 0.0898P] where P = (Fo2 + 2Fc2)/3 |
1678 reflections | (Δ/σ)max = 0.001 |
186 parameters | Δρmax = 0.20 e Å−3 |
1 restraint | Δρmin = −0.11 e Å−3 |