| Bruker Kappa APEXII CCD diffractometer | 3217 independent reflections |
| Radiation source: fine-focus sealed tube | 2493 reflections with I > 2σ(I) |
| graphite | Rint = 0.036 |
| ω and φ scan | θmax = 24.9°, θmin = 1.4° |
| Absorption correction: multi-scan (SADABS; Bruker, 1999) | h = −35→35 |
| Tmin = 0.942, Tmax = 0.971 | k = −12→12 |
| 32882 measured reflections | l = −13→14 |