Bruker SMART APEX CCD area-detector diffractometer | 1351 independent reflections |
Radiation source: fine-focus sealed tube | 786 reflections with I > 2σ(I) |
graphite | Rint = 0.017 |
φ and ω scans | θmax = 29.0°, θmin = 3.3° |
Absorption correction: multi-scan (SADABS; Sheldrick 1996) | h = −5→4 |
Tmin = 0.962, Tmax = 0.971 | k = −8→5 |
2173 measured reflections | l = −17→17 |