| Refinement on F2 | 0 restraints |
| R[F2 > 2σ(F2)] = 0.042 | H-atom parameters constrained |
| wR(F2) = 0.106 | w = 1/[σ2(Fo2) + (0.0442P)2] where P = (Fo2 + 2Fc2)/3 |
| S = 0.97 | (Δ/σ)max < 0.001 |
| 10077 reflections | Δρmax = 3.26 e Å−3 |
| 416 parameters | Δρmin = −2.53 e Å−3 |
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