Refinement on F2 | Primary atom site location: structure-invariant direct methods |
Least-squares matrix: full | Secondary atom site location: difference Fourier map |
R[F2 > 2σ(F2)] = 0.037 | Hydrogen site location: inferred from neighbouring sites |
wR(F2) = 0.047 | H-atom parameters constrained |
S = 0.96 | w = 1/[σ2(Fo2) + (0.0085P)2] where P = (Fo2 + 2Fc2)/3 |
586 reflections | (Δ/σ)max < 0.001 |
39 parameters | Δρmax = 1.41 e Å−3 |
6 restraints | Δρmin = −1.59 e Å−3 |