| Rigaku AFC10/Saturn724+ diffractometer | 3073 reflections with I > 2σ(I) |
| Radiation source: Rotating Anode | Rint = 0.029 |
| graphite | θmax = 27.5°, θmin = 3.3° |
| Detector resolution: 28.5714 pixels mm-1 | h = −14→12 |
| Multi–scan | k = −14→8 |
| 16790 measured reflections | l = −24→24 |
| 3165 independent reflections |
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