| Bruker APEXII diffractometer | 3878 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.024 |
| graphite | θmax = 30.5°, θmin = 5.2° |
| φ and ω scans | h = −13→13 |
| 27399 measured reflections | k = 0→20 |
| 4591 independent reflections | l = 0→16 |
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