Oxford Diffraction Xcalibur Sapphire2 (large Be window) diffractometer	2766 independent reflections
Radiation source: Enhance (Mo) X-ray Source	2209 reflections with I > 2σ(I)
graphite	Rint = 0.022
Detector resolution: 8.1929 pixels mm-1	θmax = 26.9°, θmin = 2.2°
ω scans	h = −5→7
Absorption correction: multi-scan (CrysAlis PRO; Oxford Diffraction, 2006)	k = −5→9
Tmin = 0.632, Tmax = 1.000	l = −45→41
5236 measured reflections