Bruker SMART area-detector diffractometer | 1796 independent reflections |
Radiation source: fine-focus sealed tube | 1356 reflections with I > 2σ(I) |
graphite | Rint = 0.042 |
φ and ω scans | θmax = 25.7°, θmin = 2.3° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −18→18 |
Tmin = 0.918, Tmax = 0.979 | k = −4→4 |
6484 measured reflections | l = −20→20 |