Bruker APEXII CCD diffractometer | 3435 independent reflections |
Radiation source: fine-focus sealed tube | 3272 reflections with I > 2σ(I) |
graphite | Rint = 0.037 |
ω and φ scans | θmax = 45.7°, θmin = 5.4° |
Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −21→21 |
Tmin = 0.179, Tmax = 0.274 | k = −20→21 |
41355 measured reflections | l = −17→17 |